| Crosbi ID | 821315 |
| Year | 2024 |
| Status | Objavljeno |
| Type | prilog u časopisu |
| Subtype | izvorni znanstveni rad |
| Authors | Alić Stolar, Jasna; Lončarić, Ivor; Ettel, Martin; Rubčić, Mirta; Štefanić, Zoran; Šekutor, Marina; Užarević, Krunoslav; Stolar, Tomislav |
| Journal | PCCP. Physical chemistry chemical physics |
| Volume | 26 |
| Issue | 6 |
| Pages | str. 4840-4844 |
| DOI | 10.1039/d3cp04364a |
| ISSN | 1463-9076 |
| EISSN | 1463-9084 |
en original Direct in situ measurement of polymorphic transition temperatures under thermo-mechanochemical conditions
For the first time, we directly measured the onset and completion temperatures of polymorphic transitions under thermo-mechanochemical conditions by simultaneous in situ synchrotron powder X-ray diffraction and temperature monitoring. We determined the thermo-mechanochemical polymorphic transition temperature in 1-adamantyl-1-diamantyl ether to be 31 °C lower than the transition temperature determined by DSC. Our findings highlight the uniqueness of thermo-mechanochemical conditions, with potential applications in polymorph screening.
en original thermo-mechanochemistry ; ball milling ; polymorphism ; diamondoids ; in situ synchrotron powder X-ray diffraction ; in situ temperature monitoring
Alić Stolar, Jasna; Lončarić, Ivor; Ettel, Martin; Rubčić, Mirta; Štefanić, Zoran; Šekutor, Marina; Užarević, Krunoslav; Stolar, Tomislav Direct in situ measurement of polymorphic transition temperatures under thermo-mechanochemical conditions // PCCP. Physical chemistry chemical physics, 26 (2024), 6; 4840-4844. doi: 10.1039/D3CP04364A
Medline Scopus Web of Science Core Collection, SCI-Exp, SSCI & A&HCI (WoSCC-SCI-Exp, SSCI, A&HCI) Web of Science Core Collection, Science Citation Index Expanded (WoSCC-SCI-Exp)