| Crosbi ID | 797030 |
| Year | 2023 |
| Status | Objavljeno |
| Type | prilog sa skupa (u zborniku) |
| Subtype | sažetak izlaganja sa skupa |
| Authors | Alić, Jasna; Etter, Martin; Rubčić, Mirta; Štefanić, Zoran; Šekutor, Marina; Užarević, Krunoslav; Stolar, Tomislav |
| Parent journal | Solid-State Science & Research 2023 : book of abstracts |
| Pages | str. 41-41 |
| ISBN | 978-953-7941-48-2 |
| Publisher | Institut Ruđer Bošković |
| Place | Zagreb |
en original Direct in situ measurement of polymorphic transition temperatures in thermo-mechanochemical reactions
Mechanochemistry is known for its efficiency and sustainability in polymorph screening. Here we present the methodology for measuring polymorphic transition temperatures in thermo-mechanochemical reactions by in situ synchrotron powder X-ray diffraction and thermal monitoring. We detected the onset and completion of the thermo-mechanochemical polymorphic transition temperature in mechanosynthesized 1-adamantyl-1-diamantyl ether, which is 27 °C lower than the corresponding differential canning calorimetry transition temperature.
en original thermo-mechanochemistry ; polymorphism ; diamondoids
Alić, Jasna; Etter, Martin; Rubčić, Mirta; Štefanić, Zoran; Šekutor, Marina; Užarević, Krunoslav; Stolar, Tomislav Direct in situ measurement of polymorphic transition temperatures in thermo-mechanochemical reactions // Solid-State Science & Research 2023 : book of abstracts / Biliškov, Nikola; Karadeniz, Bahar; Juraj Pantalon, Natalija (ur.). Zagreb: Institut Ruđer Bošković, 2023. str. 41-41