| Crosbi ID | 490278 |
| Bib IRB ID | 116465 |
| Year | 2003 |
| Status | Objavljeno |
| Type | prilog sa skupa (u zborniku) |
| Subtype | sažetak izlaganja sa skupa |
| Authors | Štefanić, Zoran ; Meden, Anton ; Kojić-Prodić, Biserka ; Makarević, Janja ; Jokić, Milan ; Žinić, Mladen |
| Parent journal | Twelfth Croatian-Slovenian crystallographic meeting : Book of Abstracts and Programme |
| Pages | str. 1-1 |
| Publisher | Hrvatska kristalografska zajednica HAZU |
| Place | Zagreb |
en original Non-merohedral twinning in the structure of rac-NN'-bis(oxalyl valinol)
A twinned crystal is an aggregate in which different domains are joined together according to a specific symmetry operation. In the case of merohedral twinning this symmetry operation belongs to the supergroup of the space group of the crystal, but not in the case of non-merohedral twins. Thus, non-merohedral twin can be easily recognized on a diffraction pattern. The title compound shows twinning which can be detected even by point detector during the data collection. The title compound (1) crystallizes as non-merohedrical twin in the triclinic space group P-1 (2). The twin law is a 180° rotation around b axes of the monoclinic supercell. The analysis of twinning law was by use of the program ROTAX[1]. Data collection was also performed using a CCD detector to resolve the problem of twinning (3). The structure was solved and refined in P-1 space group.
en original twinning; hydrogen-bonding
Štefanić, Zoran ; Meden, Anton ; Kojić-Prodić, Biserka ; Makarević, Janja ; Jokić, Milan ; Žinić, Mladen Non-merohedral twinning in the structure of rac-NN'-bis(oxalyl valinol) // Twelfth Croatian-Slovenian crystallographic meeting : Book of Abstracts and Programme. Zagreb: Hrvatska kristalografska zajednica HAZU, 2003. str. 1-1